Thermogravimetric Analysis and Differential Scanning Calorimetry

thermogravimetric analysis and differential scanning calorimetry in Massachusetts

Thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) are techniques to characterize materials in pharmaceuticals, material science, food, and petrochemicals. They measure the weight of a compound as it is heated or cooled in a controlled environment, as well as endothermic and exothermic properties, and more. TGA and DSC are comprehensive and versatile, therefore they can analyze a wide range of materials, including polymers, laminates, composites, rubbers, elastomers, and fillers.

How can you use thermogravimetric analysis and differential scanning calorimetry?

TGA can evaluate the thermal stability of a material. In a desired temperature range, if a material is thermally stable, there is no observed change of mass. TGA also reveals the upper use temperature of a material, beyond which the material will begin to degrade.

LSI offers a wide range of thermal analysis tests, including TGA, TGA-FT-IR, DSC, and mDSC:

  • temperature and heat of fusion, vaporization and crystallization
  • heat of reaction, including polymerization, oxidation and combustion
  • temperature and heat of decomposition (e.g., dehydration)
  • heat of solution, adsorption or desorption
  • specific heat, activation energy, polymer crystallinity, curing time
  • material purity, thermal and oxidative stability
  • reactivity and reaction rates
  • temperature and glass transition, softening, linear coefficient of expansion

For more info on TGA and DSC, Perkin Elmer has an excellent guide.

thermogravimetric analysis and differential scanning calorimetry in Massachusetts